Abstract: The present invention comprises preparation of Fenspiride hydrochloride (Ia) starting from N-(2-phenylethyl)-2-oxo-6-azaspiro[2.5]octane (III) by a novel method. The compound of formula (III) is converted to 4-(aminomethyl)-1-(2-phenyIethyl)piperidin-4-ol of formula (VI) either by treatment with sodium azide/ammonium chloride followed by reduction or by treating with potassium phthalimide/phthalimide followed by reaction with hydrazine hydrate to give compound of formula (VI) which is then converted to Fenspiride free base (I) of desired purity and impurity profile by subsequent treatment with carbonyl diimidazole.
Name | Date | |
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1 | 3339-mum-2010-abstract.pdf | 2018-08-10 |
2 | 3339-mum-2010-correspondence.pdf | 2018-08-10 |
3 | 3339-mum-2010-description(provisional).pdf | 2018-08-10 |
4 | 3339-mum-2010-form 1.pdf | 2018-08-10 |
5 | 3339-mum-2010-form 2(title page).pdf | 2018-08-10 |
6 | 3339-mum-2010-form 2.pdf | 2018-08-10 |
7 | 3339-mum-2010-form 3.pdf | 2018-08-10 |
8 | 3339-mum-2010-form 5.pdf | 2018-08-10 |
9 | 3339-MUM-2010-ABSTRACT(28-11-2011).pdf | 2011-11-28 |
10 | 3339-MUM-2010-CLAIMS(28-11-2011).pdf | 2011-11-28 |
11 | 3339-MUM-2010-CORRESPONDENCE(28-11-2011).pdf | 2011-11-28 |
12 | 3339-MUM-2010-DESCRIPTION(COMPLETE)-(28-11-2011).pdf | 2011-11-28 |
13 | 3339-MUM-2010-FORM 1(28-11-2011).pdf | 2011-11-28 |
14 | 3339-MUM-2010-FORM 2(28-11-2011).pdf | 2011-11-28 |
15 | 3339-MUM-2010-FORM 2(TITLE PAGE)-(28-11-2011).pdf | 2011-11-28 |
16 | 3339-MUM-2010-FORM 3(28-11-2011).pdf | 2011-11-28 |
17 | 3339-MUM-2010-FORM 5(28-11-2011).pdf | 2011-11-28 |