Abstract:
This invention relates to an improved process for the preparation of Naptha [1,8-cd] dithiole. The product is prepared from 1,8-diamino naphthalene in two simple organic transformations. In the process a diaminonaphthalene is treated with a diazotizing agent to obtain dihalo derivative of naphthalene which is farther treated with sulphur in presence of an aprotic solvent to get the product. The process has excellent yield and purity.The products rae pure do not need any further purification.
Applicants
1. COUNCIL OF SCIENTIFIC AND INDUSTRIAL RESEARCH
RAFI MARG, NEW DELHI- 110 001, INDIA
Inventors
1. KUMAR VENKATARAMAN SRINIVASAN
NATIONAL CHEMICAL LABORATORY, PUNE-411 008, MAHARSHTRA, INDIA
2. THOMAS DANIEL
NATIONAL CHEMICAL LABORATORY, PUNE-411 008, MAHARSHTRA, INDIA
3. RAJGOPAL JAGANNATH LAHOTI
NATIONAL CHEMICAL LABORATORY, PUNE-411 008, MAHARSHTRA, INDIA
4. RAMAVARMA RAJGOPAL
NATIONAL CHEMICAL LABORATORY, PUNE-411 008, MAHARSHTRA, INDIA
Specification
1. KUMAR VENKATARAMAN SRINIVASAN
NATIONAL CHEMICAL LABORATORY, PUNE-411 008, MAHARSHTRA, INDIA
2. THOMAS DANIEL
NATIONAL CHEMICAL LABORATORY, PUNE-411 008, MAHARSHTRA, INDIA
3. RAJGOPAL JAGANNATH LAHOTI
NATIONAL CHEMICAL LABORATORY, PUNE-411 008, MAHARSHTRA, INDIA
4. RAMAVARMA RAJGOPAL
NATIONAL CHEMICAL LABORATORY, PUNE-411 008, MAHARSHTRA, INDIA