Abstract: 4-Chloro, 4’-Hydroxy Benzophenone (I) was prepared in 71-72% total yield and >99.5% purity. A one pot synthesis of I by acylation of phenol with 4-Chloro, 4’-Hydroxy Benzophenone in the presence of AICI3 and workup of the reaction mass to give Crude (I) in >95% purity and Yield of 85%. Crude (I) was further purified to give>99.5% pure (I). Thus to Phenol dissolved in ODCB is added AICI3. To this is added 4-Chloro, 4’Hydroxy Benzophenone, and the whole mass maintained at 80 C for 12 hours. The reaction mass is worked up by drowning in dilute HCI solution and Crude (I) of purity>95% ppts. out. This is further purified by to give>99.5% pure material in 71-72% yield.
Year | CBR Date | CBR Number | Renwal Amount | Renwal Date | Normal Due Date | Renwal To | Renwal From | Due Date with Extension | Reneal Certificate Number |
---|---|---|---|---|---|---|---|---|---|
3rd year | 17/05/2010 | 6299 | 2000 | 17/05/2010 | 15/05/2010 | 13/12/2008 | 13/12/2007 | 15/11/2010 | 2762 |
4th year | 17/05/2010 | 6299 | 2000 | 17/05/2010 | 15/05/2010 | 13/12/2009 | 13/12/2008 | 15/11/2010 | 2762 |
5th year | 17/05/2010 | 6299 | 2000 | 17/05/2010 | 15/05/2010 | 13/12/2010 | 13/12/2009 | 15/11/2010 | 2762 |
6th year | 29/10/2010 | 12733 | 2000 | 29/10/2010 | 13/12/2010 | 13/12/2011 | 13/12/2010 | 13/06/2011 | 5631 |
7th year | 02/09/2011 | 10311 | 6000 | 02/09/2011 | 13/12/2011 | 13/12/2012 | 13/12/2011 | 13/06/2012 | 4634 |
8th year | 30/11/2012 | 16043 | 6000 | 30/11/2012 | 13/12/2012 | 13/12/2013 | 13/12/2012 | 13/06/2013 | 6226 |
9th year | 12/12/2013 | 18312 | 6000 | 12/12/2013 | 13/12/2013 | 13/12/2014 | 13/12/2013 | 13/06/2014 | 6476 |
10th year | 30/10/2014 | 16288 | 13200 | 30/10/2014 | 13/12/2014 | 13/12/2015 | 13/12/2014 | 13/06/2015 | 9076 |
11th year | 30/10/2015 | 16851 | 26400 | 30/10/2015 | 13/12/2015 | 13/12/2016 | 13/12/2015 | 13/06/2016 | 9004 |
12th year | 25/10/2016 | 32321 | 26400 | 25/10/2016 | 13/12/2016 | 13/12/2017 | 13/12/2016 | 13/06/2017 | 10211 |
13th year | 16/10/2017 | 19910 | 26400 | 16/10/2017 | 13/12/2017 | 13/12/2018 | 13/12/2017 | 13/06/2018 | 11192 |
14th year | 29/10/2018 | 23861 | 26400 | 29/10/2018 | 13/12/2018 | 13/12/2019 | 13/12/2018 | 13/06/2019 | 13809 |
15th year | 23/10/2019 | 23017 | 26400 | 23/10/2019 | 13/12/2019 | 13/12/2020 | 13/12/2019 | 13/06/2020 | 20302 |
16th year | 23/10/2020 | 27323 | 44000 | 23/10/2020 | 13/12/2020 | 13/12/2021 | 13/12/2020 | 13/06/2021 | 25318 |
17th year | 28/10/2021 | 24760 | 44000 | 28/10/2021 | 13/12/2021 | 13/12/2022 | 13/12/2021 | 13/06/2022 | 29124 |
18th year | -- | -- | -- | -- | -- | -- | -- | -- | -- |
19th year | -- | -- | -- | -- | -- | -- | -- | -- | -- |
20th year | -- | -- | -- | -- | -- | -- | -- | -- | -- |